Experiment (E), Report Form and Marking Guide |
Tutorial (T) |
Assessment |
Learning Tools |
References
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Safety notes
Course notes Reagents Table in Excel
Appendix to the manual and the yellow pages
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All homework reports are due at the start of the next E class. In-lab assignments are due at the end of the class in which they have been given. |
Lab
technique tips
Intro to drawing programs
Periodic Table
Molecular
weight calculator |
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E0 Introduction and luminescent lanthanides.
Report form for E0
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T0 Admin & general concepts of spectroscopy.
Answers to practice problems |
T0 In-class workbook
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Video on balancing the equation and stoichiometric ratios
Video on the reagents table and limiting reagent Video on calculating % yield |
Reference 1
Reference 2 |
E1 Chemically active extraction
Report template for E1 |
T1 1H NMR spectroscopy
Answers to practice problems |
E1 pre-lab is on Brightspace
E1Structured report
T1 In-class workbook |
Video on thin layer chromatography
Video on liquid-liquid extraction
Video on using the rotary evaporator
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E2 The oxidation states of cobalt
Report template for E2
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T2 IR interpretation of infrared spectra
Answers to practice problems
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E2 Structured report
T2 In-class workbook |
Video on balancing the equation and stoichiometric ratios
Video on the reagents table and limiting reagent Video on calculating % yield
Video on
bonding & magnetism Guidelines on balancing redox equations
Standard reduction potentials for common half-reactions
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Reference
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E3 Synthesis and chemistry of alkenes
Report template for E3 |
T3 1H NMR of alkenes and mixtures
Answers to practice problems |
E3 pre-lab is on Brightspace
E3 Structured report
T3 In-class workbook |
Video on setting up a distillation
Review of tlc
Video on using the ATR-IR spectrometer
Video on IR instrumentation
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E4 Titanium
Report template for E4
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T4 Titanium structural analysis |
E4 + T4 Structured report and in-lab assignments |
Titanium in solution
Transition metals, magnetism and colour
Viewing crystal structures
Point group determination |
Reference 1; Reference 2
Reference 3; Reference 4
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E5 Separation of a reaction mixture
Report template for E5
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T5 13C and DEPT-135 NMR
Answers to practice problems |
E5 pre-lab is on Brightspace
E5 Structured report
T5 In-class workbook |
Video on column chromatography
Review of tlc
Review of rotovaps
Review of ATR-IR |
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E6 Copper carboxylates
Report template for E6
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T6 Copper carboxylates IR analysis
Copy of handout data table given in class (T6)
IR spectra of free carboxylic acids (handout in class) |
E6 + T6 Structured report |
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Reference 1; Reference 2
Copper in Canada
IR spectra of free carboxylic acids (handout in class)
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E7 Selective reduction
Report template for E7
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T7 Analyses of reduction products |
E7 pre-lab is on Brightspace
E7&T7 Structured report
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Video on NMR instrumentation
Video on NMR sample prep
Review liquid-liquid extraction
Review of rotovaps
Review of ATR-IR
Video on melting ranges |
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E8 Vanadium tartrate complexes
Report form for E8 |
T8 Processing NMR spectra |
E8 Report form
T8 In-class workbook |
Video on
inorganic optical isomers
Transition metals, magnetism and colour |
Reference 1
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E10 Tin(II) or tin(IV)?
Report template for E10
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T10 Mass spectrometry
Answers to practice problems |
E10 structured report
T10 In-class workbook |
Video of how a mass spectrometer works |
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E11 The Aldol reaction
Report template for E11 |
T9 Multinuclear and spin dilute systems in NMR.
Answers to practice problems |
E11 Structured report due at end of class |
Review of ATR-IR
Review melting ranges |
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E13 Green chemistry considerations for an amide coupling reaction.
Report template for E13
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E13 interpretation continued |
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Reference 1; Reference 2; Reference 3 |